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Tris[(pentafluorophenyl)trimethylsilylamido](tetrahydrofuran)samarium(III) (2000)

Click, Damon R. ; Scott, Brian L. ; Watkin, John G.

Oxford [u.a.] : International Union of Crystallography (IUCr)

Acta crystallographica 56 (2000), S. 1095-1096

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ISSN: 1600-5759

Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001

Topics: Chemistry and Pharmacology , Geosciences , Physics

Notes: In the title complex, [Sm(C9H9F5NSi)3(C4H8O)], the Sm metal center is coordinated in a highly distorted tetrahedral geometry by the three N atoms of the amido ligands and by the O atom of the tetrahydrofuran ligand. Principal bond lengths include: Sm—N 2.299 (4), 2.339 (4) and 2.366 (4) Å, and Sm—O 2.446 (3) Å, close Sm...F contacts of 2.536 (3) and 2.556 (3) Å, and an `agostic' Sm...C interaction of 3.154 (4) Å.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1107/S0108270100008775

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