ISSN:
1551-2916
Source:
Blackwell Publishing Journal Backfiles 1879-2005
Topics:
Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
,
Physics
Notes:
We monitor the synthesis of ZrO2 colloids from dissolved ZrOCl2·8H2O using quasi-elastic light scattering and cryo-transmission electron microscopy (cryo-TEM). We investigate the effects of both precursor salt concentration and pH on the final size distribution. We find that the initial pH plays the most important role in the final particle size and yield. These trends and cryo-TEM observations help elucidate the roles of nucleation, aggregation, and recrystallization.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1111/j.1551-2916.1999.tb20067.x
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