ISSN:
1573-4803
Source:
Springer Online Journal Archives 1860-2000
Topics:
Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
Notes:
Abstract Joining of pressurelessly sintered silicon nitride ceramics was carried out using adhesive slurries in the system Y-Si-Al-O-N in a nitriding atmosphere. The effects of bonding parameters, such as joining temperature (1450–1650°C), applied pressure (0– MPa) and holding time (10–60 min), on the bond strength of joint were evaluated. A typical microstructure of the joint bonded with the optimum adhesive was investigated. The three point bend testing of joined samples with 3 × 4 × 36 mm3 in dimension was employed to study the bond strength of joints. The results show that an optimum joining process was achieved by holding at 1600°C for 30 min under an external pressure of 5 MPa and the maximum bond strength was 550 MPa, compared to 700 MPa of unbonded Si3N4 ceramic, using the adhesive having the Si3N4/(Y2O3 + SiO2 + Al2O3) ratio of 0.39. The good bond strength is attributed to the similarity in microstructure and chemical composition between joint zone and ceramic substrate. The fracture modes were classified into two types according to the values of bond strength.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1023/A:1004507124881
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