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  • 1985-1989  (12)
  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 58 (1987), S. 1811-1816 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Detailed operations of the apparatus for the stroboscopic observation of periodic phenomena at the region of line frequencies, such as the magnetic domain response, under the scanning electron microscopy are described in this paper. To achieve the stroboscopic observation at such low frequencies, a new line-sampling technique has been introduced instead of the conventional point-sampling method. In addition to the line-sampling stroboscopy, a multiframe operation is also introduced to display the stroboscopic images of different phase values simultaneously. These operations are simply realized by applying the raster separation and the blanking on the display monitor scope under the multiple line-sampling during the one-drive period. To demonstrate the ability of this simple apparatus, some results of the stroboscopic observation of magnetic domains in an Fe–Si sample under a 60-Hz drive field are also presented in this paper.
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A new method for pattern reduction in the x-ray region is proposed. In its principle was used the asymmetric Bragg reflection giving the different beamwidth in the reflected beam from the incident one. Light from an undulator line (BL-2) at the Photon Factory was used to obtain highly spatially resolved replication in reasonably short exposure time. Performed was one-dimensional demagnification of a pattern with a ratio of 1/4 in the following condition: Si 111 reflection was used where the offset angle α from the surface is 22° and the wavelength λ was 3.5 λ, which is available from the 7th harmonic of the undulator radiation. The submicron scale resist pattern was resolved.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 61 (1987), S. 3559-3561 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The temperature dependence of the coercivity (HcI)of Nd15(Fe1−xCox)77B8 and (Nd1−xDyx)15Fe77B8 sintered magnets and that of the saturation magnetization (Ms) and the anisotropy field (HA) of Nd2(Fe1−xCox)14B and (Nd1−xDyx)2Fe14B single crystals have been observed in the temperature range between 295 and 800 K. The dependence of the coercivity on the major magnetic properties of the matrix phase in the Nd-Fe-B based magnets are investigated using the μ0HA vs μ0HcI+Ms plot. It is demonstrated that this method of analysis is useful in studying the coercivity mechanism of the Nd-Fe-B based sintered magnets.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 58 (1985), S. 1606-1609 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A line-sampling multiframe stroboscopic observation system was attached to a commercial-type 200-kV scanning electron microscope for dynamic observation of ferromagnetic domains in grain-oriented 3% silicon steels with orientation near (110) [001]. This technique has enabled the individual stroboscopic image, at different phases of drive field, to be observed on a display tube simultaneously, leading to a more comprehensive understanding of core-loss characteristics of the silicon steels magnetized at commercial frequency in practical use. The observation has clearly revealed that uniform displacement of domain walls according to the alternating magnetization at commercial frequency leads to lower core losses during operation.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 63 (1988), S. 3319-3320 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Microstructure of grain-boundary regions in sintered Nd15Fe77B8 magnets has been observed under a high-resolution TEM. Crystalline Nd-rich phase is not observed at all the grain boundaries, while amorphouslike layers are observed quite often. It has also been found that no bcc phase in as-sintered samples was observed before heating the samples but heating of the samples for annealing has caused bcc microcrystals to form in the edges of the matrix phase.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 62 (1987), S. 2733-2737 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A new version for the marlowe code, which enables dynamic simulation of damage processes during ion implantation to be performed, has been developed. This simulation code is based on uses of the Ziegler–Biersack–Littmark potential [in Proceedings of the International Engineering Congress on Ion Sources and Ion-Assisted Technology, edited by T. Takagi (Ionic Co., Tokyo, 1983), p. 1861] for elastic scattering and Firsov's equation [O. B. Firsov, Sov. Phys. JETP 61, 1453 (1971)] for electron stopping. By introducing a damage function f(z)=l−exp[−ΔE(z)/Ecrit], where ΔE(z) is the deposition energy due to nuclear stopping per unit volume at depth z and Ecrit is the critical energy assessed from the experiment, the present code allows us to simulate how the crystalline structure at depth z transforms to the disordered structure, resulting in the marked change in the penetration of implanted ions as ion implantation proceeds. To examine the applicability of the present simulation code for practical ion implantation, we have performed dynamic simulations of the depth profile of implanted ions considering the changes in the crystalline structure due to disordering during ion implantations, and the results are compared with the experimental results of Mayer et al. [Can. J. Phys. 46, 664 (1968)]. The agreement between theoretical and experimental results has been found to be very good. A prediction on the dose dependence of lattice disorder for practical low-dose implantation in GaAs is also presented.
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 51 (1987), S. 376-377 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The recently developed dynamic observation technique of R. Shimizu and T. Ikuta [Appl. Phys. Lett. 44, 811 (1984)] for scanning electron microscopy, "line-sampling stroboscopy,'' was used for the observation of magnetic domains in an amorphous ferromagnetic ribbon. The image-processing technique introduced turned out to be very useful, allowing the behavior of domain walls, which is often obscured by topological contrast, to be clearly observed.
    Type of Medium: Electronic Resource
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  • 8
    ISSN: 1612-1112
    Keywords: Chiral reagent ; Amino acids ; TLC and HPLC
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary The applicability of a new chiral reagent to the resolution of amino acid enantiomers has been investigated. The new reagent, S(-)-N-1-(2-naphthylsulphonyl)-2-pyrrolidinecarbonyl chloride (NSP-C1), was synthesized by the chlorination of S(-)-N-1-(2-naphthylsulphonyl)-2-pyrrolidinecarboxylic acid which was prepared by the reaction of 2-naphthalene sulphonyl chloride with L-proline. Derivatization of the amino acids proceeds rapidly at ambient temperature and no racemization takes place during the reaction. The resolution of the diastereomeric amides was performed by TLC and normal phase HPLC. Complete resolutions were observed for the enantiomers of all amino acids examined except cysteine, cystine and histidine. The favourable UV absorption of the derivatives enabled the optical antipode to be determined down to the 0.1% level.
    Type of Medium: Electronic Resource
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  • 9
    ISSN: 0142-2421
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: The Japanese VAMAS-SCA working group is composed of 19 institutes. Three kinds of Au-Cu alloys (Au25 at%-Cu75 at%, Au50 at%-Cu50 at%, Au75 at%-Cu25 at%) were prepared, and these specimens were distributed to the members of Japanese VAMAS-SCA working group and Auger peak amplitude ratios were measured to clarify the correlation factor of different types of spectrometers. The comparison was carried out by using the relative sensitivity factor for Au and Cu. The relative sensitivity factor for lower energy varied from spectrometer to spectrometer, but that for higher energy did not vary so much. Therefore, to carry out the inter-laboratory comparison of the data, the transfer of the data of peak amplitude at higher energy should be recommended.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    Chichester [u.a.] : Wiley-Blackwell
    Surface and Interface Analysis 12 (1988), S. 161-161 
    ISSN: 0142-2421
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Type of Medium: Electronic Resource
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