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Studies on clathrasils: VII. A new clathrate compound of silica: Synthesis, crystallographic, and thermal properties (1984)

Gies, H.

Springer

Journal of inclusion phenomena and macrocyclic chemistry 2 (1984), S. 275-278

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ISSN: 1573-1111

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Abstract Using l-aminoadamantane a new type of silica host framework has been stabilized. The clathrasil is rhombohedral with a=13.887Å and c=40.989Å for the hexagonal unit cell. Heating the compound on a thermal analyser shows that from 500°C on the guest molecule evaporates. The silica framework only very slowly breaks down when heated at 1100°C for several hours yielding cristobalite. Since l-aminoadamantane stabilizes, at higher temperatures of synthesis, dodecasil 1H the new clathrasil is regarded as low temperature form for this particular guest molecule.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00663266

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