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  • 1975-1979  (1)
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    Electronic Resource
    Electronic Resource
    Springer
    Journal of chemical crystallography 9 (1979), S. 57-65 
    ISSN: 1572-8854
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences , Physics
    Notes: Abstract Orthorhombic crystals of the title compound, C7H16ClNO2SSn, belong to space groupP212121, witha = 6.658(5),b = 10.974(3),c = 17.144(5) Å, andZ = 4. The diffractometer data, measured with CuKα radiation, has been refined to anR index of 0.053 for 1110 observed terms. The geometry about the Sn atom in the monomeric complex units is distorted trigonal bipyramidal; the N and Cl atoms are in the apical positions, and the Sn lies at 0.107(1) Å from the equatorial plane. The Sn-Cl, Sn-S, and Sn-N bonds have lengths 2.523(4), 2.413(3), and 2.434(12) respectively, and the angle N-Sn is 166.9(3) °.
    Type of Medium: Electronic Resource
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