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  • Articles: DFG German National Licenses  (2)
  • 2,8-Dioxatetracyclo[3.3.3.06.0.03,10]undecan-4-ol  (1)
  • autooxidation  (1)
  • 1
    Electronic Resource
    Electronic Resource
    Synthesis and characterization of a self-crosslinkable polymer from cardanol: Autooxidation of poly(cardanyl acrylate) to crosslinked film (1993)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part A: Polymer Chemistry 31 (1993), S. 1069-1073 
    Details
    ISSN: 0887-624X
    Keywords: cardanol ; cardanyl acrylate ; self-crosslinkable polymer ; autooxidation ; hydroperoxide ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Cardanyl acrylate (CA), a monomer that yields crosslinkable copolymers, was synthesized by the reaction of cardanol with acryloyl chloride. A linear polymer was obtained by solution polymerization of the monomer in toluene using 0.8% azobisisobutyronitrile as initiator. Upon removal of solvent, the polymer undergoes crosslinking on exposure to air (or UV light) to give an insoluble transparent film. However, in bulk and suspension polymerization the polymer undergoes in situ crosslinking in the absence of any crosslinking agent. The polymer was characterized by IR, NMR, DSC, and GPC. The crosslinking reaction of soluble polymer on exposure to air at ambient conditions was explained by the hydroperoxide theory. © 1993 John Wiley & Sons, Inc.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pola.1993.080310429
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    Spectral separation of two very closely related organic compounds by 1D TOCSY (1994)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 32 (1994), S. 452-457 
    Details
    ISSN: 0749-1581
    Keywords: NMR ; 1D TOCSY ; z-Filtering ; 2,7-Dioxatetracyclo[3.3.04,9.08,11]undeca-3,6-dione ; 8,10,11-Trioxapentacyclo[5.4.1.02,6.04,11.05,9]dodecane ; 2,8-Dioxatetracyclo[3.3.3.06.0.03,10]undecan-4-ol ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The use of one-dimensional total correlation spectroscopy (1D TOCSY) combined with the z-filtration technique to generate pure phase subspectra of individual isomers from the spectrum of the corresponding mixture without any chemical separation of the mixture is described. A straightforward spectral assignment is achieved for the isomers obtained on lithium aluminium hydride reduction of 2,7-dioxatetracyclo[3.3.04,9.08,11] undeca-3,6-dione (dilactone) by studying the subspectrum of each isomer as a function of the propagation time of magnetization through the network of coupled protons.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1260320804
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    Paper (German National Licenses)
    Fulltext
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