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  • 1
    Electronic Resource
    Electronic Resource
    New York, NY [u.a.] : Wiley-Blackwell
    Biospectroscopy 1 (1995), S. 29-36 
    ISSN: 1075-4261
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Biology , Physics
    Notes: The FT-Raman vibrational spectrum of a child's deciduous exfoliated tooth has been analysed and the spectral features assigned to hydroxyapatite and protein. Comparisons made with older teeth from a Romano-British burial site (∼ 2k years) and fossilised animal teeth (∼ 1 M-70 M years) indicate that the organic protein component has disappeared with interment, whereas spectroscopic features due to the inorganic phosphatic matrix are common to all samples, modern and ancient. The application of the technique to the non-destructive analysis of archaeological samples and the recording of spectra from interred samples without detriment from fluorescent material is demonstrated. © 1995 John Wiley & Sons, Inc.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 1 (1968), S. 169-187 
    ISSN: 0030-493X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The mass spectra of guanidine and ten of its derivatives have been studied under both high and low resolution conditions. Evidence was detected for the migration of methyl groups, the formation of intermediate three-membered ring structures and decompositions involving expulsion of N. with release of kinetic energy.
    Additional Material: 13 Ill.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 3 (1970), S. 1009-1021 
    ISSN: 0030-493X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The n-alkanes, propane to heptane, have been studied in a modified MS-9 mass spectrometer under conditions that enabled the daughter ions, resulting from metastable fragmentation processes occurring in the first field free region, to be observed with high sensitivity. The precursor ions in these fragmentations have been identified unambiguously and a general fragmentation scheme for the n-alkanes is proposed. The mass spectrometer incorporated a variable width monitor slit and narrow settings of this slit improved the energy resolution so that fine structure could be observed in some of the ‘metastable peaks’. The implications of this fine structure are discussed.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 5 (1971), S. 303-310 
    ISSN: 0030-493X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Benzene, toluene, phenol, diphenyl ether and the three isomeric dihydroxy-benzenes have been examined using an MS-9 mass spectrometer under conditions that allowed only ions having twice the normal amount of kinetic energy to be detected. These ions are, in fact, singly charged ions arising from charge exchange reactions of doubly charged ions of the same mass, occuring in the first field free region of the Spectrometer. It is argued that the spectra obtained yield essentially the distribution of doubly charged ions in the source region. These ‘doubly charged ion’ mass spectra are compared with the normal singly charged ion spectra of the compounds and the implications of the significant differences that are found, are discussed.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 18 (1983), S. 506-508 
    ISSN: 0030-493X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 30 (1995), S. 793-796 
    ISSN: 1076-5174
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Certain of the “meta-stable peaks” in mass spectra are abnormally wide. This extra width is shown to be associated with release of kinetic energy during fragmentation. Methods are presented for measuring this energy release and values are given for various transitions in the spectra of aromatic nitro compounds.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 11 (1988), S. 289-291 
    ISSN: 0935-6304
    Keywords: Supercritical fluid chromatography, SFC ; Capillary columns ; Restrictor ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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  • 8
    ISSN: 0935-6304
    Keywords: Supercritical fluid extraction, SFE ; Supercritical fluid chromatography, SFC ; Fourier transform infrared microspectrometry, FTIR ; Narrow-bore capillary column ; Polycyclic aromatic compounds, PAC ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The combination of supercritical fluid extraction, high resolution capillary supercritical fluid chromatography, and Fourier transform infrared microspectrometry is described for the separation and identification of polycyclic aromatic hydrocarbons in a coal tar pitch. The variable solvating power of the supercritical fluid was utilized to selectively fractionate the sample. The fluid extract was decompressed through a frit restrictor into the sample cavity of a cooled microvalve injector, where the analytes were deposited and concentrated for subsequent chromatographic analysis. Several of the analytes separated in the chromatograph were collected on a potassium bromide disc at a solvent elimination inter-face for subsequent infrared analysis involving the use of an infra-red microscope accessory. The spectra obtained show the power of this detection technique for distinguishing between isomers.
    Additional Material: 11 Ill.
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 4 (1981), S. 421-422 
    ISSN: 0935-6304
    Keywords: Gas chromatography ; Capillary columns ; Unstable flavor compound ; Comparison of fused silica, glass, and metal columns ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    Chichester [u.a.] : Wiley-Blackwell
    Journal of Raman Spectroscopy 25 (1994), S. 95-98 
    ISSN: 0377-0486
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Fourier transform Raman spectra of human keratotic biopolymers were obtained. The spectra from skin stratum corneum, callus, nail and hair were fluorescence free and the samples did not degrade during analysis. Assignments consistent with the vibrational wavenumbers were made to characterize the molecular and conformational nature of the samples. The principal structural dissimilarities were in the sulphur content of tissues containing hard keratin (hair and nail) and soft keratin (stratum corneum and callus).
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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