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Enantioselective Preparation of 2,4-Disubstituted Azetidines (2000)

Marinetti, Angela ; Hubert, Philippe ; Genêt, Jean-Pierre

Weinheim : Wiley-Blackwell

Liebigs Annalen 2000 (2000), S. 1815-1820

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ISSN: 1434-193X

Keywords: Asymmetric synthesis ; Palladium-catalysed couplings ; Palladacycles ; Chemistry ; General Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: ---Chiral C2-symmetric N-benzylazetidines have been conveniently prepared from optically pure anti-1,3-diols without loss of enantiomeric purity. N-Debenzylation led to the corresponding N-unsubstituted azetidines, which were then subjected to palladium-catalysed coupling reactions with aryl bromides to afford chiral N-arylazetidines. (R,R)-N-Benzyl-2,4-dimethylazetidine has been employed in the synthesis of a new cyclopalladated complex, which can be used, for instance, as a chiral recognition agent for phosphorus ligands.

Additional Material: 1 Tab.

Type of Medium: Electronic Resource

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