ISSN:
0018-019X
Keywords:
Chemistry
;
Organic Chemistry
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
Crystals of azacyclododecane hydrochloride (a = 13.77, b = 5.07, c = 9.67 Å, α = 109°26′, β = 90°22′, γ = 101°16′) and hydrobromide (a = 13.53, b = 5.19, c = 9.45 Å, α = 99°40′, β = 83°57′, γ = 98°28′) are isomorphous, space group P1, Z = 2. The conformation of the 12-membered ring has been established from three-dimensional X-ray analysis. It corresponds closely to the idealized model with 422-symmetry, containing 8 syn-clinal and 4 anti-periplanar partial conformations.
Additional Material:
7 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/hlca.19640470504
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