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Determination of fluoride in urinary calculi using a quantitative microdiffusion method (1988)

Wandt, M. A. E. ; Rodgers, A. L.

Springer

Urological research 16 (1988), S. 431-436

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ISSN: 1434-0879

Keywords: Urinary calculi ; Trace elements ; Fluoride ; Diffusion ; Ion selective electrode

Source: Springer Online Journal Archives 1860-2000

Topics: Medicine

Notes: Summary A microdiffusion method for the separation of fluoride from other ions in urinary calculi has been developed, tested and assessed. The procedure involves digestion at 75°C of samples with silicone-impregnated mixtures of nitric and perchloric acids in a specially designed diffusion cell and determination of the diffused fluoride with an ion-sensitive electrode. Several test samples were used to assess the recovery, accuracy and reproducibility of the procedure. Results for 20 stones of Indian origin are presented and discussed.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00280024

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