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Acyclic stereochemical analysis by NMR spectroscopy (1987)

Kleinpeter, E. ; Meusinger, R. ; Duschek, Ch. ; [et al.]

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 25 (1987), S. 990-995

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ISSN: 0749-1581

Keywords: NMR ; γ-chloropropyl methyl ethers ; Vicinal H,H coupling constants ; Steric compression Conformation ; Diastereomer assignment ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The diastereomers of a series of substituted γ-chloropropyl methyl ethers with up to three chiral centres have been assigned by 1H/13C NMR spectroscopy from vicinal H,H coupling constants and the steric compression within the carbon skeleton (γ-gauche effect). The necessary conformational study was carried out with the help of theoretically estimated steric 1,3-parallel interaction energies.

Additional Material: 3 Tab.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260251114

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