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  • 1
    Electronic Resource
    Electronic Resource
    Mechanical relaxations in polyamides (1971)
    New York : Wiley-Blackwell
    Journal of Polymer Science Part A-2: Polymer Physics 9 (1971), S. 867-886 
    Details
    ISSN: 0449-2978
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Dynamic mechanical measurements were carried out as a function of temperature (-100 to + 180°C) and frequency (3.5 to 110 cps) for a series of aliphatic terpolyamides, nylon 6 and nylon 12. Effect of crosslinking with toluene diisocyanate, of absorbed water, and of frequency are used to estimate the statistical segment length associated with the α′ relaxation. The effects of variations in the aliphatic chain length in the repeating unit on the temperature of the α′ relaxation are examined by means of copolymer rules with a view to explaining the reported insensitivity of the glass transition temperature of these polymers to changes in (CH2)/(amide) group ratio. From the estimated length of the segmental motion associated with the α′ relaxation it is inferred that in a series of polyamides of the type nylon X or nylon X,Y (where X or Y = 3, 4, 5, 6, etc.) there should be a relatively small change in the temperature of the α′ transition for those polyamides having X or Y less than about 45. Experiments which are intended to establish the position of the crystalline α-γ transition are discussed.
    Additional Material: 14 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1971.160090508
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    A similarity criterion of the optimal process in melt spinning (1980)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 25 (1980), S. 1165-1178 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Experimental and simulation studies of optimization of the melt spinning process were carried out for nylon 6 fibers. The experiment and process simulation demonstrated that one criterion that can be applied in scaling up an optimized melt spinning process is to achieve the similar real time history of temperature and deformation rate in the spinway. Some aspects of the experiments and process simulation are discussed, together with the results of real time history analysis for a case of nylon 6 spinning.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1980.070250619
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    Paper (German National Licenses)
    Fulltext
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