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  • 1
    Digitale Medien
    Digitale Medien
    Springer
    Colloid & polymer science 277 (1999), S. 382-387 
    ISSN: 1435-1536
    Schlagwort(e): Key words Enamel conditioning ; Surface analysis ; Benzoic acid ; Analytical electron microscopy ; X-ray photoelectron spectroscopy
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie , Maschinenbau
    Notizen: Abstract  The effects of surface pretreatment on the topography and composition of dental enamel surfaces of extracted bovine teeth have been investigated by scanning electron microscopy and X-ray photoelectron spectroscopy. Surface pretreatment with a solution of benzoic acid in acetone does not change the topography of the surface; it leads to enrichment of calcium and, to a lesser extent, phosphorus at the enamel surface. The higher adhesion strength reported between enamel surfaces pretreated with benzoic acid in acetone and glass ionomer cement might be explained in terms of a greater number of chemical bonding sites due to the enrichment of calcium and phosphorus at the surface.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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  • 2
    Digitale Medien
    Digitale Medien
    Chichester [u.a.] : Wiley-Blackwell
    Surface and Interface Analysis 16 (1990), S. 504-509 
    ISSN: 0142-2421
    Schlagwort(e): Chemistry ; Polymer and Materials Science
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Physik
    Notizen: The effects of non-metallic inclusions on the microstructure of as-deposited C-Mn weld metals have been investigated in a series of welds produced using different electrode coatings to obtain inclusions of different chemical compositions. The inclusions were analysed on carbon extraction replicas or in thin foils in a 120 kV (scanning) transmission electron microscope (TEM (STEM)) equipped with energy dispersive x-ray microanalysis facilities. Both x-ray microanalysis and convergent beam diffraction techniques, with probe sizes down to 10 nm, were used to characterize the inclusions and the inclusion/matrix interfaces.It was found that the ‘cores’ of the inclusions were mainly oxides, such as MnSiO3 or MnAl2O4. The surfaces of the inclusions were either coated with thin layers of copper sulphide, or mixtures of copper sulphide and titanium carbonitride when both copper and titanium were present as impurities in the welds. Effects of non-metallic inclusions on weld metal microstructure are discussed with respect to the above-mentioned coatings and the heterogeneous nucleation of the fine acicular ferrite microconstituent.
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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