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  • 1
    ISSN: 1438-1168
    Keywords: Tantalum ; Niobium ; Titanium ; Columbite ; Rutile ; Mineralogy ; Geochemistry ; Pegmatite ; Austria ; Ostalpen
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences
    Description / Table of Contents: Zusammenfassung Titan-Ferrocolumbit ist ein seltenes Akzessorium in den Spodumenpegmatiten der Weinebene, Kärnten, Österreich. Er enthält entmischten niobhaltigen Rutil und selten Einschlüsse von möglicherweise primärem Zinnstein. Die Zusammensetzung des TitanFerrocolumbits ist relativ homogen und weist die folgenden Elementverhältnisse auf. Mn/(Mn + Fe) 0,24 – 0,33, Ta/(Ta + Nb) 0,09 – 0,13 (Atomverhältnisse) und 0,47 – 0,88 Ti pro 12 Kationen (2,7 - 5,0Gew.%TiO2). Natürlich auftretende Kristalle sind strukturell merklich ungeordnet und erlangen durch Erhitzen einen höheren Ordnungsgrad. Die Mn/(Mn + Fe) sowie Ta/(Ta + Nb) Verhältnisse des niobhaltigen Rutil betragen 0,00 – 0,04 bzw. 0,26 – 0,38. Der niobhaitige Rutil ist im Vergleich zu Mn- und Nb-führendem Ferrocolumbit an Fe, Ta, Ti und Sn angereichert.—Die Seltenheit von Nb, Ta-Oxiden in den spodumenführenden Pegmatiten der südlichen Ostalpen steht in Übereinstimmung mit ihrer Zugehörigkeit zum Albit-Spodumen Typ der selten-Element-führenden Pegmatite (rare-element pegmatites).
    Notes: Summary Titanian ferrocolumbite is a rare accessory mineral in the spodumene-bearing pegmatites at Weinebene, Carinthia, Austria. It contains abundant exsolved niobian rutile and scarce inclusions of cassiterite that may be primary. The titanian ferrocolumbite is relatively homogeneous with Mn/(Mn + Fe) 0.24–0.33, Ta/(Ta + Nb) 0.09–0.13 (atomic ratios) and 0.47–0.88 Ti per 12 cations (2.7–5.0 wt.% TiO2). Natural specimens are considerably disordered but become more ordered on heating. Niobian rutile has Mn/(Mn + Fe) 0.00–0.04 and Ta/(Ta + Nb) 0.26–0.38; it concentrates Fe, Ta, Ti and Sn relative to the Mn- and Nb-enriched ferrocolumbite. The overall scarcity of Nb, Ta-oxide minerals in the spodumene-bearing pegmatites of southern Ostalpen conforms to their general features ranking them with the albite-spodumene type of rare-element pegmatites.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    Mineralogy and petrology 41 (1989), S. 53-63 
    ISSN: 1438-1168
    Keywords: Tantalum ; niobium ; tantalite ; tapiolite ; mineralogy ; geochemistry ; pegmatite ; Ostalpen ; Austria
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences
    Description / Table of Contents: Zusammenfassung In einem Pegmatit von Spittal a.d. Drau, Kärnten, treten enge Verwachsungen von Ferrotantalit und Ferrotapiolit auf. Diese werden von Muskovit, Albit, Rauchquarz, Zinnstein sowie-in mikroskopischem Masstab-von Uranmikrolith und Zirkon begleitet. Die Textur der Verwachsungen lässt Rekristallisation erheblichen Ausmasses erkennen, die die primären Merkmale weitgehend auslöscht. Weder eine gemeinsame Auskristallisation der beiden Mineralphasen noch eine Bildung durch Entmischung kann mit Sicherheit erkannt werden. Trotz einander kreuzender Verbindungslinien, die einen Hinweis auf Ungleichgewicht darstellen, zeigen die Zusammensetzungen des Ferrotantalits und des Ferrotapiolits lediglich geringe Schwankungsbreiten: Mn/(Mn + Fe) 0,08–0,11, Ta/(Ta + Nb) 0,53–0,57 für den Ferrotantalit beziehungsweise 0,01–0,04 und 0,84–0,89 für den Ferrotapiolit. Dies gilt insbesondere für den Vergleich mit Zusammensetzungen solcher Mineralphasen mit jenen von Fundarten, die primäre Verwachsungstrukturen aufweisen. Bis zu einem gewissen Ausmass ist diese homogene Zusammensetzung möglicherweise auf die Rekristallisation zurück zuführen. Diese Rekristallisation könnte auch den hohen strukturellen Ordnungsgrad der beiden Mineralphasen erklären. An anderen Fundorten zeigen diese Minerale strukturell merklich geringeren Ordnungsgrad. Intensive metamorphe überprägung, wie sie für die Pegmatite in den südlichen Ostalpen und insbesondere für jenen von Spittal typisch sind, kann wahrscheinlich als Ursache der Rekristallisationsphänomene der Ta-Nb-Sn Mineralparagenese angenommen werden.
    Notes: Summary Intimate intergrowths of ferrotantalite and ferrotapiolite occur in a pegmatite in Spittal a.d. Drau, Carinthia. They are associated with muscovite, albite, smoky quartz, cassiterite, and microscopic uranmicrolite, zircon and uraninite. An assemblage of secondary uranium minerals is also present, generated by extensive alteration and leaching of the uranmicrolite and zircon. Textures of the ferrotantalite-ferrotapiolite intergrowths suggest considerable recrystallization that obliterated most of their primary features; neither coprecipitation nor exsolution can be recognized with certainty. Despite intersecting tielines indicating disequilibrium, the ferrotantalite and ferrotapiolite compositions show very restricted ranges (Mn/(Mn + Fe) 0.08–0.11, Ta/(Ta + Nb) 0.53–0.57 for ferrotantalite, and 0.01–0.04, 0.84–0.89 for ferrotapiolite, respectively), particularly in comparison with compositions from other localities featuring primary textures. A degree of compositional equilibration could have been attained during recrystallization. This process may also explain the high level of structural order characterizing both minerals; they are considerably disordered in other localities. Extensive deformation typical of pegmatites in the southern Ostalpen in general, and specifically of the Spittal pegmatite, is probably responsible for the recrystallization phenomena in the Ta, Nb, Sn-bearing mineral assemblage.
    Type of Medium: Electronic Resource
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  • 3
    ISSN: 1572-9702
    Keywords: Tetranychus urticae ; Panonychus ulmi ; Petri dish bioassay ; propargite ; precision
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology
    Notes: Abstract The effect of interval space between the concentration (symmetric or geometric), number of concentrations and overall sample sizes were investigated using a Petri dish bioassay, the miticide propargite and two spider mites species. The precision (width of the 95% confidence intervals) of the LC50 and LC90 estimates was shown to be influenced by the test design and total sample size The results suggest that a symmetric five-concentration design using a minimum total sample size of 480 mites is required to produce reliable LC estimates using the Petri dish method. Asymmetric designs did not increase the reliability of LC estimates. When less than 480 test subjects are available, a symmetric three-concentration design would give adequate LC estimates, but the precision would be less than with a five-concentration design.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Springer
    Experimental and applied acarology 19 (1995), S. 549-570 
    ISSN: 1572-9702
    Keywords: Fluvalinate ; Tetranychus urticae ; Panonychus ulmi ; toxicity ; dispersal ; development rate ; oviposition ; sublethal effects
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology
    Notes: Abstract Four fluvalinate formulations differed in their residual toxicity to female two-spotted spider mite (TSM), Tetranychus urticae adults; the emulsifiable concentrate (EC) was the most toxic. In contrast, there was little difference in toxicity between the formulations with the European red mite (ERM) Panonychus ulmi with the exception of the EC formulation which was the least toxic. Fluvalinate 2F caused minimal (〈10%) TSM and ERM egg mortality. Fluvalinate 2F was more toxic and caused greater larval dispersal for the TSM compared to the ERM at the field concentration and below. The toxicity of fluvalinate 2F to TSM and ERM protonymphs, deutonymphs and adults was low, approximately 〈20% at field concentration. Dispersal was the main response to fluvalinate and this was positively correlated with increasing concentration. The combined mortality and dispersal LC50 was five times lower for ERM protonymphs and adults, but 11 times higher for ERM deutonymphs compared to equivalent TSM life stages. Fluvalinate 2F reduced TSM development from the protonymph and deutonymph stages to a greater extent compared to the ERM. The mortality response to fluvalinate 2F was unaffected by host type (peach or apple) for the TSM whereas ERM mortality was higher on apple compared to peach. TSM dispersal was higher from apple compared to peach whereas ERM dispersal was similar on both host types. Oviposition by both mite species was lower on apple than peach leaves. A 1 h exposure to fluvalinate 2F reduced ERM oviposition for 12 days.
    Type of Medium: Electronic Resource
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