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Digitale Medien

A combined differential scanning calorimeter-optical video microscope for crystallization studies (1997)

Hey, J. M. ; Mehl, P. M. ; MacFarlane, D. R.

Springer

Journal of thermal analysis and calorimetry 49 (1997), S. 991-998

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Details

ISSN: 1572-8943

Schlagwort(e): cryo-microscopy ; crystallization ; DSC ; ICE ; microscopy

Quelle: Springer Online Journal Archives 1860-2000

Thema: Chemie und Pharmazie

Notizen: Abstract A simultaneous differential scanning calorimeter (DSC)-optical video microscope instrument has been developed. The instrument development included slight modifications to the sample head of a Perkin-Elmer DSC-7, along with the use of a CCD camera and magnifying lenses. The instrument permitted simultaneous following of optical and thermal events during isothermal and non-isothermal DSC experiments. The DSC curves were almost identical to those given by a standard DSC-7. The operational temperature range of the instrument is between −160 to 600°C. The capabilities of the DSC-video microscope are illustrated by examples of ice crystallization data in aqueous solutions of glycerol and dimethyl sulphoxide.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1007/BF01996785

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