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Synthesis and structure of (±)-4-O-methanesulfonyl-myo-inositol 1,3,5-orthoformate (2000)

Praveen, T. ; Puranik, V.G. ; Shashidhar, M.S.

Springer

Journal of chemical crystallography 30 (2000), S. 605-609

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ISSN: 1572-8854

Keywords: Inositol ; cyclitol ; C8H12O8S ; signal transduction ; hydrogen bonding

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract Racemic 4-O-methanesulfonyl-myo-inositol 1,3,5-orthoformate was prepared by methanolysis of racemic 2,4-di-O-benzoyl-4-O-methanesulfonyl-myo-inositol 1,3,5-orthoformate, in the presence of triethylamine. The diol crystallizes in space group P212121 with cell dimensions a = 6.094(1), b = 6.502(2), c = 25.947(3) Å, V = 1028.1(4) Å, Z = 4. The molecular crystals show both intra- and intermolecular O—H···O short contacts. The methine and the methyl hydrogens are involved in several C—H···O interactions.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1023/A:1011314512066

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