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ESR investigation of the dimerization of some dithiazolidinyl radicals (1987)

Fairhurst, Shirley A. ; Stewart, Neil J. ; Sutcliffe, Leslie H.

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 25 (1987), S. 60-64

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Details

ISSN: 0749-1581

Schlagwort(e): ESR ; Energetics of dimerization ; dithiazolidiny radicals ; Chemistry ; Analytical Chemistry and Spectroscopy

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: Four types of dithiazolidin-2-yl radical were selected for dimerization measurements in solution. The radicals had different types of substituents and/or different amounts of strain; ESR measurements for a new dithiazolidinyl radical prepared from trans-cyclooctene are presented. Toluene, diethyl ether and chloroform were used as solvents. Radical concentration measurements incorporated corrections for the variation of the Q of the spectrometer cavity with solvent and temperature. It was found that ΔH⊖ for the dimerization process is dependent only on the radical structure.

Zusätzliches Material: 2 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/mrc.1260250115

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