ISSN:
1573-9171
Keywords:
fullerene C60
;
extraction
;
thermal stability
;
TG
;
DSC
;
phase transitions
Source:
Springer Online Journal Archives 1860-2000
Topics:
Chemistry and Pharmacology
Notes:
Abstract Extraction of fullerenes from carbon soot by trichloroethylene has been studied. We have found that C60 forms a solvate with trichloroethylene (C60 · C2HCl3:a=31.31(1);b= 10.156(4);c=10.146(4) Å;V=3228.6 Å3,Z=4,d calc=1.752 g cm−3, orthorhombic symmetry). Its thermal stability has been studied using TG and DSC. A phase transition of the first order at 167 K has been detected.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF00698240
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