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Digitale Medien

X-ray structure of tricyclohexylmethyl chloride (1996)

Gillies, D. G. ; Luff, S. ; Smith, G. W. ; [weitere]

Springer

Journal of chemical crystallography 26 (1996), S. 539-542

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Details

ISSN: 1572-8854

Schlagwort(e): Tricyclohexylmethyl chloride ; structure ; tricylohexylmethyl

Quelle: Springer Online Journal Archives 1860-2000

Thema: Geologie und Paläontologie , Physik

Notizen: Abstract The X-ray crystallographic structure of tricyclohexylmethyl chloride, a precursor of the tricyclohexylmethyl radical, has been determined. Colourless tablets of C19H33Cl crystallized from hexane/chloroform in the orthorhombic space group Pnma, with cell dimensions a=10.725(3),b=15.670(3),c=10.168(3) Å;V=1708.8(1.3) Å3;Z=4. 1586 reflections withI〉3 σ(I), and 302 with zero intensity, on refinement gaveR=0.046,R w=0.076. The three cyclohexyl rings are arranged to give the molecule a plane of symmetry containing the central C−H axis. The large volume per nonhydrogen atom, of about 21.3 Å3, is close to values found in the crystal structures of analogous tricyclohexyl compounds.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1007/BF01668412

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