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  • 1
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 93 (1981), S. 1-10 
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Es werden die Synthese und Eigenschaften eines Resacetophenon (2,4-Dihydroxiacetophenon)-Formaldehyd Harzes beschrieben. Das mittlere Molekulargewicht des Harzes, durch Dampfdruckosmometrie und wasserfreie konduktometrische Titration bestimmt, beträgt 2500 bzw. 2200 g/mol.Von diesem Harz wurden Cu(II)-, Ni(II)- und Co(II)-Chelate hergestellt. Die Elementaranalyse der Chelate ergab ein Verhältnis Metall : Ligand von 1:2. Aus den Reflexionspektren der Chelate konnte geschlossen werden, daß Ni(II)- und Co(II)-Chelate eine tetraedrische Struktur haben, während Cu(II)-Chelate eine quadratisch-ebene Struktur zeigen. Infrarotuntersuchungen zeigen, daß die Metalle über den Sauerstoff der Carbonyl-und Phenolgruppe gebunden sind. Auch die Anwesenheit von Methylenbrücken ist aus den IR-Messungen zu erkennen. Die thermischen Eigenschaften des Harzes und seiner Metallchelate werden diskutiert.
    Notes: Synthesis and properties of a resacetophenone-formaldehyde resin are described. The number average molecular weight of the resin determined by vapour pressure osmometry and nonaqueous conductometric titration is 2500 and 2200 g/mol, respectively.Cu(II), Ni(II) and Co(II) chelates of the resin were prepared. The elemental analysis of chelates indicated a metal to ligand ratio 1:2. From the diffuse reflectance spectra of the chelates it could be concluded that Ni(II) and Co(II) chelates have a tetrahedral structure while Cu(II) chelate has a square planar structure. Infrared spectral studies showed that the metals are co-ordinated through the oxygen of the carbonyl and phenolic groups. The presence of methylene bridges was also indicated from IR spectral studies. The thermal properties of the resin and its metal chelates are discussed.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 93 (1981), S. 11-17 
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Resacetophenon-Formaldehyd-Harze erwiesen sich für verschiedene Metallionen als selektiv komplexierende Ionenaustauscherharze. Zur Bestimmung der Selektivität der Metallionenaufnahme wurde eine Gleichgewichts-batch-Methode angewandt. Die Methode beinhaltet die Messung der Verteilung eines gegebenen Metallions zwischen einer wäßrigen Lösung und dem Harz. Die Untersuchung wurde über einen weiten pH-Bereich und in Medien verschiedener Ionenstärke durchgeführt.
    Notes: The resacetophenone-formaldehyde (RAP-F) resin showed to be a selective chelating ion-exchange resin for certain metal ions. A batch equilibration method was used in the study of the selectivity of metal ion uptake. The method involved the measurement of distribution of a given metal ion between an aqueous solution and the resin. The study was carried out over a wide pH range and in media of various ionic strengths.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 105 (1982), S. 75-81 
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Resacetophenonoxim-Formaldehyd-Harze erwiesen sich für verschiedene Metallionen als selektiv komplexierende Ionenaustauscherharze. Zur Bestimmung der Selektivität wurde eine Gleichgewichts-batch-Methode angewandt. Die Methode beinhaltet die Messung der Verteilung eines gegebenen Metallions zwischen einer wäßrigen Lösung und dem Harz. Die Untersuchung wurde in einem weiten pH-Bereich und in Medien verschiedener Ionenstärke durchgeführt.
    Notes: Resacetophenoneoxime-formaldehyde resins showed to be selective chelating ion exchange resins for certain metal ions. A batch equilibrium method was used in the study of the selectivity of metal ion uptake. The method involved the measurement of distribution of a given metal ion between an aqueous solution and the resin. The study was carried out over a wide pH range and in media of various ionic strengths.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Chemistry Edition 20 (1982), S. 205-212 
    ISSN: 0360-6376
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: In this paper the synthesis and properties of resacetophenone oxime-formaldehyde resin are described. The number-average molecular weights of the resin determined by vapor-pressure osmometry and nonaqueous conductometric titration are 2200 ± 10% and 2500 g/mol, respectively. Cu(II), Ni(II), and Co(II) chelates of the resin were prepared. Elemental analysis of the chelates indicates a metal to ligand ratio of 1:2. The diffuse reflectance spectra and magnetic moments of Ni(II) and Co(II) chelates show tetrahedral structure, whereas Cu(II) chelate shows a square planar structure. Infrared spectral studies show that the metals are coordinated through the nitrogen of the oximino group and oxygen of the phenolic group. The presence of methylene bridges is also indicated by IR spectral studies. The thermal behavior of the resin and its metal chelates are also discussed.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    s.l. : American Chemical Society
    Journal of the American Chemical Society 47 (1925), S. 863-867 
    ISSN: 1520-5126
    Source: ACS Legacy Archives
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    Springer
    Diabetologia 27 (1984), S. 370-372 
    ISSN: 1432-0428
    Keywords: Type 2 diabetes ; HLA antigens ; Papua New Guinea ; diabetes genetics
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary HLA phenotypes were studied in 57 Type 2 (non-insulin-dependent) diabetic Papuan patients and the results compared with control subjects of the same Austronesian origin. An association was found between disease and BW62, a split antigen of B15, with corrected probability significant at the 5% level. The frequencies of B13 and BW22 were also increased in diabetic patients but the differences were not statistically significant. Although it has been postulated that Melanesian communities have protection against diabetes, they have a high frequency of BW62, which would imply, from the association found in this study, that susceptibility to Type 2 diabetes has yet to become manifest in them.
    Type of Medium: Electronic Resource
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  • 7
    ISSN: 1432-0428
    Keywords: Rat ; hepatic pyruvate dehydrogenase complex ; blood lactate ; glucose ; insulin
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary At birth, hepatic ‘active’ and ‘dichloracetate-activated’ pyruvate dehydrogenase complex activities in the newborn of normal, mildly diabetic, and severely diabetic rats were similar. The ‘active’ and ‘dichloracetate-activated’ pyruvate dehydrogenase complex activities increased significantly during the first 2 and 6 postnatal h, respectively in the three groups of neonates (p〈0.05). The greatest increase in both ‘active’ and ‘dichloroacetate-activated’ pyruvate dehydrogenase complex activity was observed in the neonates of mildly diabetic rats. Administration of glucose or insulin at birth to the newborn of normal rats caused a significant increase in the percentage of ‘active’ pyruvate dehydrogenase complex activity within 1 h (p〈0.01). Similar treatment caused no significant increases in the newborn of severely diabetic rats. The transient increases in ‘active’ pyruvate dehydrogenase complex activity in the neonates of normal and diabetic rats were consistent with rapid disappearance of blood lactate during the first hours of postnatal life.
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    Springer
    European radiology 7 (1997), S. 1454-1462 
    ISSN: 1432-1084
    Keywords: Key words: Pleural diseases ; Empyema ; Fibrinolysis ; Biopsy ; thoracentesis ; Pneumothorax
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Abstract. This is a review of the role of radiological intervention in the pleural space. It discusses the radiological management of effusions, empyemas (including the use of fibrinolytic agents), pneumothoraces and pleural thickening.
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    Springer
    European journal of clinical pharmacology 44 (1993), S. 63-67 
    ISSN: 1432-1041
    Keywords: Mexiletine ; Debrisoquine hydroxylation phenotype ; pharmacokinetic ; variability
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Medicine
    Notes: Summary Marked interindividual variation has been observed in the pharmacokinetics of the antiarrhythmic agent mexiletine. The fact that its urinary excretion is dependent on urinary pH may account, in part, for such variation. The influence that genetic differences in hepatic metabolism of the debrisoquine-type may have on mexiletine pharmacokinetics was considered in this study. The pharmacokinetics and urinary excretion of mexiletine (250 mg administered intravenously) were investigated in 5 rapid extensive metabolisers (EM), 5 slow EM and 5 poor metabolisers (PM) of debrisoquine, under conditions of controlled urinary pH. Mexiletine disposition kinetics was found to be altered in PM individuals. These subjects showed higher total area under the curve (AUC), (15.7 versus 8.16 μg · h · ml−1) prolonged elimination half-lives (in serum and urine) (serum: 18.5 versus 11.6 h, urine: 19.2 versus 11.7 h) and lower total clearance values compared with EM (216 versus 450 ml · min−1). In this respect, slow EM individuals generally presented intermediate values of those pharmacokinetic parameters. A higher incidence of adverse-effects was also observed among slow EM and PM subjects. It is concluded that genetic differences in mexiletine oxidation of the debrisoquine-type have an influence on its observed pharmacokinetic variability. The clinical consequences are discussed.
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    USA/Oxford, UK : Blackwell Science Ltd
    Cephalalgia 16 (1996), S. 0 
    ISSN: 1468-2982
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Medicine
    Notes: We compared data from 243 patients with episodic migraine (EM) and 132 patients with chronic daily headache (CDH). We divided the matter group into those with tension-type headache only (CDH Type 1) and those with headaches having migrainous features (CDH Types 2+3) and compared each with the EM group and all three groups with one another. CDH Type l patients differed from those in the other groups by virtue of gender (more often male) and mean age at headache onset (older). The CDH Types 2+3 and EM groups differed only in that the former were more likely to have undergone a brain-imaging study. These data suggest that CDH Type 1 may represent a distinct headache syndrome, while CDH Types 2+3 closely resemble episodic migraine.
    Type of Medium: Electronic Resource
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