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Some observations on the WATR method for water suppression at 80 MHz (1987)

Dickinson, Noel A. ; Lythgoe, Ronald E. ; Waigh, Roger D.

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 25 (1987), S. 996-997

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Details

ISSN: 0749-1581

Schlagwort(e): 1H NMR ; WATR ; Water suppression ; Ammonium chloride ; Guanidinium chloride ; Buffer salts ; Chemistry ; Analytical Chemistry and Spectroscopy

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: The WATR method for water suppression in 1H NMR spectroscopy has been evaluated at 80 MHz, using both ammonium and guanidinium chloride, with and without the addition of buffer salts. The pH of maximum effect has been found to depend on field strength and to be markedly affected by buffer salts, particularly phosphates. Provided that the pH is carefully controlled the method is simple and effective.

Zusätzliches Material: 5 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/mrc.1260251115

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