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  • 1
    Digitale Medien
    Digitale Medien
    Thermistor ceramic with negative temperature coefficient based on Zn7Sb2O12: An inverse spinel-type phase (2002)
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 81 (2002), S. 451-453 
    Details
    ISSN: 1077-3118
    Quelle: AIP Digital Archive
    Thema: Physik
    Notizen: The electric properties of the semiconductor ceramic Zn7Sb2O12 were investigated by impedance spectroscopy. The grain resistance exhibits a thermistor behavior with negative temperature coefficient. Two regions on the resistance curve were identified. Each region shows a different thermistor characteristic parameter (β), which is equal to 3170 and 3845 °C, at measurement temperatures up to 350 °C and above 450 °C, respectively. The temperature coefficient of the resistance (α) was derived being equal to −2.59×10−2 °C−1 and −1.89×10−2 °C−1, at 350 and 450 °C, respectively. The anomalous behavior of the resistance is further evidence of phase transition phenomenon. © 2002 American Institute of Physics.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1063/1.1494101
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  • 2
    Digitale Medien
    Digitale Medien
    Microstructural development of ZnO varistor during reactive liquid phase sintering (1996)
    Springer
    Journal of materials science 31 (1996), S. 5391-5398 
    Details
    ISSN: 1573-4803
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Maschinenbau
    Notizen: Abstract The microstructural evolution, grain growth and densification for the varistor systems ZnO-Bi2O3 (ZB), ZnO-Bi2O3-Sb2O3 (ZBS), ZnO-Bi2O3-Sb2O3-MnO-Cr2O3-CoO (ZBSCCM) were studied using constant heating rate sintering, scanning electron microscopy (SEM) andin situ phase formation measurement by high temperature X-ray diffraction (HT-XRD). The results showed that the densifying process is controlled by the formation and decomposition of the Zn2Bi3Sb3O14 pyrochlore (PY) phase for the ZBS and ZBSCCM systems. The addition of transition metals (ZBSCCM system) alters the formation and decomposition reaction temperatures of the pyrochlore phase and the morphology of the Zn7Sb2O12 spinel phase. Thus, the spinel grains act as inclusions and decrease the ZnO grain growth rate. Spinel grain growth kinetics in the ZBSCCM system showed ann value of 2.6, and SEM and HT-XRD results indicate two grain growth mechanisms based on coalescence and Ostwald ripening.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1007/BF01159308
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  • 3
    Digitale Medien
    Digitale Medien
    The effect of heating rate on the sintering of agglomerated NaNbO3 powders (1998)
    Springer
    Journal of materials science 33 (1998), S. 4791-4795 
    Details
    ISSN: 1573-4803
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Maschinenbau
    Notizen: Abstract The effect of heating rate on the sintering of agglomerated NaNbO3 powders, processed by the polymeric precursors method, was studied. The results showed that the presence of agglomerated powder leads to a heterogeneous microstructure, with bimodal grain size distribution, after sintering. Using a high heating rate, the sintering of agglomerated particles was inhibits, leading to a homogeneous microstructure, with single grain size distribution.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1023/A:1004422111613
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