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Experimental design optimization of the analysis of gasoline by capillary gas chromatography (1997)

Durand, Jean Pierre ; Gautier, Serge ; Robert, Eric ; [weitere]

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 20 (1997), S. 289-294

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Details

ISSN: 0935-6304

Schlagwort(e): Capillary gas chromatogrophy ; Experimental design optimization ; Gasoline analysis ; Chemistry ; Analytical Chemistry and Spectroscopy

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: An optimization procedure for multi-step temperature programmed capillary GC was investigated for the detailed hydrocarbon analysis of gasoline. A set of twelve responses, represented by the value of the resolution of the most difficult separations, was selected from several isothermal analyses. The variation of these responses versus the temperature programming conditions was then modeled using a Doehlert matrix for experimental design. Optimal experimental conditions for the twelve responses were then obtained from a response surface optimization. The predicted and experimental resolutions were in good agreement.

Zusätzliches Material: 7 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/jhrc.1240200509

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