Skip to main content
SpringerLink
Log in

Synthesis and crystal structure of 1-phenyl-3-methylthio-4-imino-5-allyl-pyrazolo[3,4-d]pyrimidine

  • Note
  • Published:
Journal of Chemical Crystallography Aims and scope Submit manuscript

Abstract

The title compound 1-phenyl-3-methylthio-4-imino-5-allyl-pyrazolo[3,4-d]pyrimidine, C15H15N5S, has been synthesized and characterized by x-ray diffraction: orthorhombic, space group Pbca, with a = 17.3480(9), b = 8.5022(5), c = 19.8132(11) Å. Z = 8, V = 2922.4(3) Å3. The compound shows a fully delocalized pyrazolo[3,4-d]pyrimidine system with a sp2 hybridization of the N(4) atom.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

References

  1. Bendich, A.; Russell, P.J., Jr.; Fox, J.J. J. Am. Chem. Soc. 1954, 76, 6073.

    Google Scholar 

  2. Kobayashi, S. Chem. Pharm. Bull. 1973, 21, 941.

    Google Scholar 

  3. Prabhaker, Y.S.; Bhakuni, D.S. Indian J. Biochem. Biophys. 1990, 27, 342.

    Google Scholar 

  4. Zooroob, Hannti H.; Elzahab, M. Abou; Mogib, Abdel; et al. Arzneim.-Forsch. 1997, 47, 958.

    Google Scholar 

  5. Tominaga, Y.; Honakawa, Y.; Hara, M.; et al. J. Heterocycl. Chem. 1990, 27, 775.

    Google Scholar 

  6. Poli, T.; Vicentini, C.B.; Brandolini, V.; et al. Pestic. Sci. 1989, 25, 161.

    Google Scholar 

  7. Wren, Heather N. US5, 770, 601.

  8. Giri, S; Shukla, A.K., Nizamuddin. J. Indian Chem. Soc. 1990, 67, 153.

    Google Scholar 

  9. Sasada, Y. Molecular and Crystal Structures. In Chemistry Handbook, 3rd edition; The Chemical Society of Japan, Maruzen: Tokyo, 1984.

    Google Scholar 

  10. Hanefeld, Ulf.; Rees, Charles W.; White, Andrew J.P.; Williams, David J. J. Chem. Soc. Perkin Trans. 1996, 1, 1545.

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Institute of Elemento-organic Chemistry, Nankai University, Tianjin, 300071, China

    Weiqiang Chen & Linhong Weng

  2. State Key Laboratory of Elemento-organic Chemistry, Nankai University, Tianjin, 300071, China

    Guiyu Jin

Authors
  1. Weiqiang Chen
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Linhong Weng
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Guiyu Jin
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Chen, W., Weng, L. & Jin, G. Synthesis and crystal structure of 1-phenyl-3-methylthio-4-imino-5-allyl-pyrazolo[3,4-d]pyrimidine. Journal of Chemical Crystallography 29, 1291–1293 (1999). https://doi.org/10.1023/A:1009565209312

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1023/A:1009565209312

Search

Navigation