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Study on retention behavior of peropyrene-type polycyclic aromatic hydroccrbons with various bonded stationary phases in reversed-phase liquid chromatography

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Summary

The retention behavior of 15 peropyrene-type polycyclic aromatic hydrocarbons was investigated on various bonded stationary phases in reversed-phase liquid chromatography. On diphenyl and naphthylethyl bonded phases, high correlations were obtained between the molecular polarizability of solutes and their retention. However, very low or no correlations were found on various octadecyl bonded phases. These facts are discussed by using the electrostatic interaction concept between the solutes and the stationary phase. We conclude that these observations are due to two reasons: the difference in the degree of planarity of polycyclic aromatic hydrocarbons and the high ability of planarity recognition of octadecyl bonded phases.

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Author notes

  1. H. Lamparczyk

    Present address: Medical Academy, Gdansk, Poland

Authors and Affiliations

  1. School of Materials Science, Toyohashi University of Technology, 440, Toyohashi, Japan

    K. Jinno, T. Ibuki & H. Lamparczyk

  2. Gifu Prefectural Tajimi Hospital, 506, Tajimi, Japan

    M. Okamoto

  3. Kyoto Institute of Technology, 606, Kyoto, Japan

    N. Tanaka

  4. Chevron Research Company, 94802-0627, Richmond, CA, USA

    J. C. Fetzer & W. R. Biggs

Authors
  1. K. Jinno
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  2. T. Ibuki
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  3. H. Lamparczyk
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  4. M. Okamoto
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  5. N. Tanaka
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  6. J. C. Fetzer
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  7. W. R. Biggs
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Jinno, K., Ibuki, T., Lamparczyk, H. et al. Study on retention behavior of peropyrene-type polycyclic aromatic hydroccrbons with various bonded stationary phases in reversed-phase liquid chromatography. Chromatographia 25, 483–486 (1988). https://doi.org/10.1007/BF02324817

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  • DOI: https://doi.org/10.1007/BF02324817

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