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Consequence of diluting modified β-cyclodextrins in a side-chain crown ether polysiloxane and in a side-chain liquid-crystalline polysiloxane-containing crown ether as stationary phases in capillary gas chromatography

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This paper investigates the possibility of using a sidechain crown ether polysiloxane (PDB-14-C4) and a side-chain liquid-crystalline polysiloxane-containing crown ether (PSC-3) as matrices for peralkylated β-CD employed as stationary phases. Three columns, coated with PSC-3 + permethylated β-CD, PDB-14-C4 + permethylated β-CD and PDB-14-C4 + perethylated β-CD were characterized by gas chromatography. The column efficiencies, phase transitions, and selectivities were measured and compared.

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Authors and Affiliations

  1. Department of Applied Chemistry and Fine Chemical Engineering, College of Chemical Engineering, Xi'an Jiaotong University, 710049, Shaanxi Prov., P.R. China

    P. Jing

  2. Department of Chemical Engineering, Beijing Institute of Technology, 100081, Beijing, P.R. China

    R. -N. Fu, R. -J. Dai, J. -L. Ge & J. -L. Gu

  3. Department of Environmental Science, Wuhan University, 430072, Wuhan, P.R. China

    Z. Huang & Y. Chen

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  1. P. Jing
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  2. R. -N. Fu
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  3. R. -J. Dai
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  4. J. -L. Ge
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  5. J. -L. Gu
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  6. Z. Huang
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  7. Y. Chen
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Jing, P., Fu, R.N., Dai, R.J. et al. Consequence of diluting modified β-cyclodextrins in a side-chain crown ether polysiloxane and in a side-chain liquid-crystalline polysiloxane-containing crown ether as stationary phases in capillary gas chromatography. Chromatographia 43, 546–550 (1996). https://doi.org/10.1007/BF02293008

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  • DOI: https://doi.org/10.1007/BF02293008

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