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Evaluation of Kinetic Data for Crystallization of Tio2 Prepared by Hydrolysis Method

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Abstract

The formation of TiO2 prepared by hydrolysis method was presented. Thermodynamics and kinetics of anatase crystallization reaction were investigated. Differential method of kinetic data evaluation in non-isothermal conditions according toKissinger, Ozawa and Kazeev-Yerofeev was applied. Starting, crystallized and thermally treated powders were determined using X-ray powder diffraction analysis. The characteristic parameters (the activation energy, constant rate and formal kinetic order of reaction) of TiO2 formation were calculated using DSC data.

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Authors and Affiliations

  1. Center for Multidisciplinary Studies, University of Belgrade, Belgrade, Yugoslavia

    B. D. Stojanović, Z. V. Marinković & G. O. Branković

  2. Faculty of Technology and Metallurgy, Skopje, Macedonia

    E. Fidančevska

Authors
  1. B. D. Stojanović
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  2. Z. V. Marinković
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  3. G. O. Branković
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  4. E. Fidančevska
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Stojanović, B.D., Marinković, Z.V., Branković, G.O. et al. Evaluation of Kinetic Data for Crystallization of Tio2 Prepared by Hydrolysis Method. Journal of Thermal Analysis and Calorimetry 60, 595–604 (2000). https://doi.org/10.1023/A:1010107423825

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  • DOI: https://doi.org/10.1023/A:1010107423825

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