Abstract
The mass spectra of the appropriate 4-ethyl derivatives, which provide the determination of the configuration of the 4 position in the initial alcohols, are registered in the chromato-mass spectrometric investigation of mixtures of the stereoisomeric 4-vinyl-trans-decahydroquinol-4-ols using a microreactor for hydrogenation; the microreactor is placed before or after the chromatographic column.
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Communication 13 of the series “Reaction chromato-mass spectrometry.” For Communication 12, see [1].
Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 9, pp. 1215–1217, September, 1986
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Mikaya, A.I., Zaikin, V.G., Ushakova, R.L. et al. Investigation of stereoisomers of 4-alkenyl-trans-decahydroquinol-4-ols in mixtures by the method of reaction chromato-mass spectrometry. Chem Heterocycl Compd 22, 983–985 (1986). https://doi.org/10.1007/BF00478130
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DOI: https://doi.org/10.1007/BF00478130