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Synthesis and alkylation of 9-ethoxy-1H-pyrrolo[3,2-b]quinoline

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

9-Ethoxy-1H-pyrrolo[3,2-b]quinoline has been synthesized by the hydrogenation of 2-[2-(N,N-dimethylamino)vinyl]-3-nitro-4-ethoxyquinoline using Raney nickel. Alkylation using N,N-dimethylchloroethylamine and hydrolysis with HBr gave two isomers whose structures were established using PMR and mass spectrometry.

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Literature Cited

  1. R. G. Glushkov, N. K. Davydova, N. P. Solov'eva, and N. B. Marchenko, Khim. Geterotsikl. Soedin., No. 1, 135 (1987).

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  2. V. V. Takhisov, Practical Mass Spectrometry of Organic Compounds, Leningrad State University, Leningrad (1977).

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Authors and Affiliations

  1. S. Ordzhonikidze All-Union Chemico-pharmaceutical Research Institute, 119815, Moscow

    N. K. Davydova, N. P. Solov'eva, V. V. Chistyakov, N. B. Marchenko & R. G. Glushkov

Authors
  1. N. K. Davydova
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  2. N. P. Solov'eva
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  3. V. V. Chistyakov
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  4. N. B. Marchenko
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  5. R. G. Glushkov
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 5, pp. 633–635, May, 1989.

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Davydova, N.K., Solov'eva, N.P., Chistyakov, V.V. et al. Synthesis and alkylation of 9-ethoxy-1H-pyrrolo[3,2-b]quinoline. Chem Heterocycl Compd 25, 528–530 (1989). https://doi.org/10.1007/BF00482499

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  • DOI: https://doi.org/10.1007/BF00482499

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