Conclusions
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1.
The compound Pd(PPh3)2CHCl3 was prepared by the reaction of Pd(PPh3)4 with chloroform.
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2.
The IR and Raman spectra of the product have been studied and a structure proposed.
Literature cited
P. Fitton and J. E. McCeon, Chem. Comm., 4 (1968).
P. Fitton, M. P. Johnson, and J. E. McCeon, Chem. Comm., 6 (1968).
F. Cariati, R. Ugo, and F. Bonati, Inorg. Chem.,5, 1128 (1966).
H. Singer and G. Wilkinson, J. Chem. Soc., (A) 1516 (1968).
I. M. Boorman and A. J. Carty, Inorg. and Nucl. Chem. Letters,2, 101 (1968).
G. E. Coates and C. Parkin, J. Chem. Soc. (1963).
K. Kohlrausch, Combination Scattering Spectra [Russian translation], IL (1952).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 12, pp. 2854–2855, December, 1969.
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Kaliya, O.L., Temkin, O.N., Kirchenkova, G.S. et al. Oxidative coupling of chloroform with tetrakis(triphenylphosphine)palladium. Russ Chem Bull 18, 2690–2691 (1969). https://doi.org/10.1007/BF00912581
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DOI: https://doi.org/10.1007/BF00912581