Skip to main content
Log in

X-ray structure of 1,3-adamantane dicarbonamide

  • Published:
Journal of Chemical Crystallography Aims and scope Submit manuscript

Abstract

The X-ray crystal structure of 1,3-adamantane-dicarbonamide has been determined. Colourless, cube shaped crystals of C12H18N2O2 crystallize in the monoclinic space group C2/c (#15) with cell dimensionsa=7·934(3),b=15·543(3),c=9·404(2) Å, β=93.63°;V=1157.4(5) Å3 andZ=4.1074 unique reflections withI net >2.00σ(I) on refinement afforded values ofR=0.039 andR w =0.040.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Steudel, R. (Ed.)The Chemistry of Inorganic Ring Systems Elsevier: Amsterdam, 1992.

    Google Scholar 

  2. Bridson, J.N.; Copp, S.B.; Schriver, M.J.; Zhu, S.; Zaworotko, M.J..Can. J. Chem. 1994,72, 1143–1153.

    Google Scholar 

  3. Leser, J.; Rabinovich, D.Acta Cryst. 1978,B34, 2264–2269.

    Google Scholar 

  4. Ermer, O..J. Amer. Chem. Soc. 1988,110, 3747–3754.

    Google Scholar 

  5. Prelog, V.; Seiwerth.Chem. Ber. 1941,74, 1769.

    Google Scholar 

  6. Novakov, I.A.; Kulev, I.A.; Radchenko, S.S.; Birznieks, K.A.; Boreko, E.I.; Vladyko, G.V.; Korobchenko, P.A..Khim.-Farm. Zh. 1987,21, 454–458. Morozov, P.A.; Morozova, N.K.; Il'yasov, A.V.Zh. Strukt. Khim. 1983,24, 127–128. Shvekhgeimer, G.A.; Kuz'micheva, L.K.Khim. Geterotsikl. Soedin. 1976, 1654–1657.

    Google Scholar 

  7. Furniss, B.S.; Hannaford, A.J.; Smith, P.W.G.; Tatchell, A.R.Vogel's Textbook of Practical Organic Chemistry (5th ed.); John Wiley and Sons: New York, 1989.

    Google Scholar 

  8. Gilmore, C.J..J. Appl. Cryst. 1984,17, 42–46, Beurskens, P.T. DIRDIF technical report 1984/1, Nijmegen, 1984.

    Google Scholar 

  9. TEXSAN-TEXRAY, Structure Analysis Package, Molecular Structure Corporation, 1985.

  10. Cromer, D.T.; Waber, J.T..International Tables for X-Ray Crystallography Vol. IV; The Kynoch Press: Birmingham, 1974, Table 2.2A.

    Google Scholar 

  11. Johnson, C.K.. ORTEPII. Report ORNL-5138. Oak Ridge National Laboratory, TN, 1976.

    Google Scholar 

  12. March, J..Advanced Organic Chemistry (3rd Ed.) John Wiley and Sons: New York, 1985; p. 19, and references therein.

    Google Scholar 

  13. Etter, M.C.; Urbanczyk-Lipkowsk, Z.; Zia-Ebrahimi, M.; Panunto, T.W..J. Amer. Chem. Soc. 1990,112, 8415–8426.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Bridson, J.N., Schriver, M.J. & Zhu, S. X-ray structure of 1,3-adamantane dicarbonamide. J Chem Crystallogr 25, 11–14 (1995). https://doi.org/10.1007/BF01666187

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF01666187

Key Words

Navigation