Abstract
The X-ray crystal structure of 1,3-adamantane-dicarbonamide† has been determined. Colourless, cube shaped crystals of C12H18N2O2 crystallize in the monoclinic space group C2/c (#15) with cell dimensionsa=7·934(3),b=15·543(3),c=9·404(2) Å, β=93.63°;V=1157.4(5) Å3 andZ=4.1074 unique reflections withI net >2.00σ(I) on refinement afforded values ofR=0.039 andR w =0.040.
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References
Steudel, R. (Ed.)The Chemistry of Inorganic Ring Systems Elsevier: Amsterdam, 1992.
Bridson, J.N.; Copp, S.B.; Schriver, M.J.; Zhu, S.; Zaworotko, M.J..Can. J. Chem. 1994,72, 1143–1153.
Leser, J.; Rabinovich, D.Acta Cryst. 1978,B34, 2264–2269.
Ermer, O..J. Amer. Chem. Soc. 1988,110, 3747–3754.
Prelog, V.; Seiwerth.Chem. Ber. 1941,74, 1769.
Novakov, I.A.; Kulev, I.A.; Radchenko, S.S.; Birznieks, K.A.; Boreko, E.I.; Vladyko, G.V.; Korobchenko, P.A..Khim.-Farm. Zh. 1987,21, 454–458. Morozov, P.A.; Morozova, N.K.; Il'yasov, A.V.Zh. Strukt. Khim. 1983,24, 127–128. Shvekhgeimer, G.A.; Kuz'micheva, L.K.Khim. Geterotsikl. Soedin. 1976, 1654–1657.
Furniss, B.S.; Hannaford, A.J.; Smith, P.W.G.; Tatchell, A.R.Vogel's Textbook of Practical Organic Chemistry (5th ed.); John Wiley and Sons: New York, 1989.
Gilmore, C.J..J. Appl. Cryst. 1984,17, 42–46, Beurskens, P.T. DIRDIF technical report 1984/1, Nijmegen, 1984.
TEXSAN-TEXRAY, Structure Analysis Package, Molecular Structure Corporation, 1985.
Cromer, D.T.; Waber, J.T..International Tables for X-Ray Crystallography Vol. IV; The Kynoch Press: Birmingham, 1974, Table 2.2A.
Johnson, C.K.. ORTEPII. Report ORNL-5138. Oak Ridge National Laboratory, TN, 1976.
March, J..Advanced Organic Chemistry (3rd Ed.) John Wiley and Sons: New York, 1985; p. 19, and references therein.
Etter, M.C.; Urbanczyk-Lipkowsk, Z.; Zia-Ebrahimi, M.; Panunto, T.W..J. Amer. Chem. Soc. 1990,112, 8415–8426.
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Bridson, J.N., Schriver, M.J. & Zhu, S. X-ray structure of 1,3-adamantane dicarbonamide. J Chem Crystallogr 25, 11–14 (1995). https://doi.org/10.1007/BF01666187
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DOI: https://doi.org/10.1007/BF01666187