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Natural product chemistry, part 100: The structure of carissone, C15H24O2

Naturstoffchemie, 100. Mitt.: Die Struktur des Carissons, C15H24O2

  • Organische Chemie Und Biochemie
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Summary

C15H24O2,M=236.2, monoclinic, P 21,a=7.229(7),b=14.925 (9),c=6.235 (9) Å, β=92.40 (9)°,V=672.1 Å3,T=−133 °C,Z=2,D x=1.17 g cm−3. The X-ray diffraction analysis of this sesquiterpenoid fromCarissa opaca confirmed the previously proposed constitution of the isolate and, furthermore, allowed precise NMR assignment.

Zusammenfassung

C15H24O2,M=236.2, monoklin, P 21,a=7.229 (7),b=14.925 (9),c=6.235 (9) Å, β=92.40 (9)°,V=672.1 Å3,T=−133 °C,Z=2,D x=1.17 g cm−3. Die Röntgenstrukturanalyse dieses Sesquiterpenoids ausCarissa opaca bestätigte die bereits vorgeschlagene Struktur und erlaubte ferner eine genaue NMR-Zuordnung.

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Authors and Affiliations

  1. Institute of Pharmaceutical Chemistry, Westfalian Wilhelms-University, Hittorfstrasse 58-62, D-W-4400, Münster, Germany

    Johannes Reisch & Raouf A. Hussain

  2. Institute of Inorganic Chemistry, Westfalian Wilhelms-University, Wilhelm-Klemm-Strasse 8, D-W-4400, Münster, Germany

    Bernt Krebs & Mechtild Dartmann

Authors
  1. Johannes Reisch
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  2. Raouf A. Hussain
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  3. Bernt Krebs
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  4. Mechtild Dartmann
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Reisch, J., Hussain, R.A., Krebs, B. et al. Natural product chemistry, part 100: The structure of carissone, C15H24O2 . Monatsh Chem 121, 941–944 (1990). https://doi.org/10.1007/BF00808958

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  • DOI: https://doi.org/10.1007/BF00808958

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