“Near magic angle” sample spinning in NMR spectra of molecules oriented in individual and mixed liquid crystals of opposite diamagnetic anisotropies
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Advances in NMR Studies of Liquid Crystals
2004, Annual Reports on NMR SpectroscopyCitation Excerpt :These dipolar coupling constants are important for the study of conformational equilibria of flexible chain(s) in LC. Long range 2H13C dipolar coupling constants have been obtained from 1D 13C spectra of monodeuterated LC.69,245,246 For example, the proton-decoupled 13C NMR spectrum of a monodeuterated 4′-(1-deuteropentyloxy)-4-biphenylcarbonitrile (5OCB-d1) gives nine 2H13C dipolar coupling constants for carbon ranging from one to six bonds from the deuterium nucleus.247
Variable angle sample spinning NMR in liquid crystals
1994, Progress in Nuclear Magnetic Resonance SpectroscopySide-band intensities in the deuterium magnetic resonance spectra of oriented molecules spinning near the magic angle
1988, Chemical Physics LettersReconstruction of two-dimensional spectra from one-dimensional projections - Examples from solid state NMR
2014, Journal of the Indian Institute of ScienceSpinning Liquid Crystalline Samples
2007, eMagRes
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