Ligand influence on the Mössbauer isomer shift and the quadrupole splitting in some related iron complexes
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Syntheses and characterizations of α-iminopyridine compounds (alkylNCHpy)<inf>2</inf>Fe(L/X<inf>n</inf>), and an assessment of redox non-innocence
2013, PolyhedronCitation Excerpt :In general, the isomer shifts for all species can be considered reasonable for low spin Fe(II) (typically -0.2 to 0.4) [46,47], although the ordering is somewhat peculiar. On the high end of the list is [{κ-N,N′-neoPeNCH(2-pyridyl)}3Fe][OTf]2 (8-P-OTf), whose δ = 0.37 and ΔEQ = 0.47 values are similar to related compounds such as Wieghardt’s [([{κ-N,N′-PhNCMeCMeNH)3Fe]2+ (δ = 0.37, ΔEQ = 0.54), and tris-pyridine complexes [(bipy)3Fe][X]n (n = 2, X = ClO4−, δ = 0.37, ΔEQ = 0.48; n = 1, X = SO42−, δ = 0.41, ΔEQ = 0.37) [48–51]. Since the field strengths along each axis are basically the same, the quadrupole splittings are relatively small, and the isomer shifts are essentially equivalent.
Characterization of three members of the electron-transfer series [Fe(pda)<inf>2</inf>]<sup>n</sup> (n = 2-, 1-, 0) by spectroscopy and density functional theoretical calculations [pda = Redox non-innocent derivatives of N,N′-bis(pentafluorophenyl)-o-phenylenediamide(2-, 1<sup>.</sup>-, 0)]
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