Synthesis and immunoreactivity of poly(acrylamide) copolymers containing C-3- and C-7-modified, carboxyl-reduced, 4-O- and 5-O-phosphorylated K
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2000, Carbohydrate ResearchCitation Excerpt :Orthoester rearrangement in the presence of substoichiometric amounts of trimethylsilyl trifluoromethanesulfonate [16] furnished exclusively the α-allyl glycoside 14 (74%). Deprotection of 14 by Zemplén de-O-acylation and subsequent alkaline hydrolysis of the methyl ester gave the previously known sodium allyl d-glycero-α-d-talo-oct-2-ulopyranosidonate (15, 93%) [17]. Radical addition of cysteamine hydrochloride to the allyl group afforded the corresponding 3-(2-aminoethylthio)propyl glycoside 16 (65%).
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