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Crystal structure of the twinned tetramethylurea adduct of 2-phenyl-1,3-dioxa-2-borolane-4,5-dione

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Abstract

The title compound crystallizes in the monoclinic space groupP21/c. Twinning occurs between domains sharing thehk0 zone. The indices of imprecise intensity data were interpreted successfully. A subset of these data could be corrected and used in structure determination together with single-crystal intensity data of the predominant domain, whereas the remaining superposition data were excluded from refinement. Structure solution converged at satisfactory values ofR=0.082,R w=0.074. The structure consists of isolated Lewis acid base adducts.

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Authors and Affiliations

  1. Institut für Anorganische Chemie, Technische Hochschule Aachen, Professor-Pirlet-str. 1, D-52074, Aachen, Germany

    Stephan Neyses, Peter Paetzold & Ulli Englert

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  1. Stephan Neyses
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  2. Peter Paetzold
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  3. Ulli Englert
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Neyses, S., Paetzold, P. & Englert, U. Crystal structure of the twinned tetramethylurea adduct of 2-phenyl-1,3-dioxa-2-borolane-4,5-dione. Struct Chem 5, 51–55 (1994). https://doi.org/10.1007/BF02278695

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  • DOI: https://doi.org/10.1007/BF02278695

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