Summary
This paper describes the gas chromatographic separation of the mixture of di- and mono-O-isopropylidene-D-glucose and D-glucose as their trimethylsilyl derivatives. The use of OV-101 as liquid phase provides a complete separation for the all components in the mixture. Quantative analysis was performed using xylitol as the internal standard for di- and mono-O-isopropylidene-D-glucose, and sorbitol as the internal standard for α-and β-glucose.
This is a preview of subscription content, log in via an institution to check access.
Similar content being viewed by others
References
E. W. Kircher, Anal. Chem.32, 1103 (1960).
E. J. Hedgley, O. Meresz, W. G. Overend, R. Renie, Chem. Ind. 1960, 938.
R. Novina, Kem. Ind.29, 107 (1980).
R. Novina, Chromatographia15, 241 (1982).
R. Novina, Kem. Ind.28, 589 (1979).
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Novina, R. Gas-liquid chromatography of isopropylidene-glucose and glucose as their trimethylsilyl derivatives. Chromatographia 18, 21–22 (1984). https://doi.org/10.1007/BF02279458
Received:
Accepted:
Issue Date:
DOI: https://doi.org/10.1007/BF02279458