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Vibrational spectra and conformation of 2,3-diiodobuta-1,3-diene (1993)

Karlsson, A. ; Klaeboe, P. ; Nielsen, C. J.

Chichester [u.a.] : Wiley-Blackwell

Journal of Raman Spectroscopy 24 (1993), S. 299-302

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ISSN: 0377-0486

Keywords: Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology , Physics

Notes: Raman and infrared spectra of the very unstable compound 2,3-diiodobuta-1,3-diene were recorded in the crystalline state at low temperatures in the spectral ranges 3300-10 and 4000-200 cm-1, respectively. Owing to a rapid polymerization rate at room temperature, only incomplete IR data were obtained of the sample in CCl4 solution. The vibrational spectra were analysed and support a planar anti conformer present in the cyrstal. The vibrational assignments are presented, supported by force constant calculations.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/jrs.1250240506

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