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Analytik Atypischer Fettsäuren in biologischen Matrizes (1985)

Pöurschmann, J. ; Pörschmann, S. ; Liebetrau, L. ; [et al.]

Berlin : Wiley-Blackwell

Acta Biotechnologica 5 (1985), S. 297-308

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ISSN: 0138-4988

Keywords: Life Sciences ; Life Sciences (general)

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Process Engineering, Biotechnology, Nutrition Technology

Notes: By combined application of chemical pretreatments, capillary gas-chromatography and mass spectrometry it was possible to enlighten the structure of atypical fatty acids with hydroxy groups and cyclopropane rings under the use of only a few of reference substances.The direct alkaline saponification of the sample with liberation of fatty acids and following methylation with boron trifluoride/methanol or diazomethane was proved to be the best method regarding to precision and speed of the sample cleanup.

Additional Material: 5 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/abio.370050318

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