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Asterane, XXII. Synthese eines doppelten Tetraasterans: Nonacyclo[10.8.0.02,11.04,9.04,19.06,17.07,16.09,14.014,19]eicosan (1991)

Hoffmann, Volker Thomas ; Musso, Hans

Weinheim : Wiley-Blackwell

Berichte der deutschen chemischen Gesellschaft 124 (1991), S. 103-109

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ISSN: 0009-2940

Keywords: Asteranes ; Cage compounds ; Chemistry ; Inorganic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Asteranes, XXII1). - Synthesis of a Double Tetraasterane: Nonacyclo[10.8.0.02,11.04,9.04,19.06,17.07,16.09,14.014,19]eicosane1,4,5,8-Tetrahydronaphthalene-2,3-dicarboxylic anhydride (9) is dimerized by UV light in dioxane yielding four isomeric [2 + 2] adducts whose methyl ester derivatives are elucidated spectroscopically. The structures of the major products 14 and 16 have been confirmed by X-ray structure analysis. Degradation of the carboxylic groups of 14 afforded the title compound 5.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/cber.19911240118

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