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An Improved Synthesis of 1,4-Benzo- and 1,4-Naphthoquinones Bearing Active Substituents (1985)

Syper, Ludwik ; Kloc, Krystian ; Młochowski, Jacek

New York, NY : Wiley-Blackwell

Journal für Praktische Chemie/Chemiker-Zeitung 327 (1985), S. 808-822

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ISSN: 0021-8383

Keywords: Chemistry ; Organic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The synthesis of 1,4-benzoquinones and 1,4-naphthoquinones 3a-j carrying substituents such as methoxyl, ally or oxiranyl was substantially improved. The 1-methoxy-4-methoxy-methyloxy 2a-d, g-k or 1,4-bis(methoxymethyloxy) derivatives 2e-f were used, as a substrates instead of 1,4-dimethoxy derivatives 1a-j hitherto used and they were oxidized with silver(II) dipicolinate. Among numerous examples, the synthesis a of new analog of ubiquinone 3d with the oxiranyl substituent, being a new bioactivated alkylating agent, is reported.

Additional Material: 4 Tab.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/prac.19853270513

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