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Silanes on magnesium chloride studied by solid-state 29Si-NMR spectroscopy (1993)

Clayden, Nigel J. ; Jones, Peter J. V.

Bognor Regis [u.a.] : Wiley-Blackwell

Journal of Polymer Science Part A: Polymer Chemistry 31 (1993), S. 2835-2838

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ISSN: 0887-624X

Keywords: NMR ; MAS ; silanes ; Ziegler-Natta ; Chemistry ; Polymer and Materials Science

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: 29Si cross-polarisation NMR was used to study the interaction between silanes and MgCl2 when co-milled. Large changes are seen for the 29Si chemical shift of the silane between the silane in solution and in the solid complex. Interpretation of the differences in chemical shift are hindered by the absence of an adequate semi-empirical theory. The 29Si chemical shift tensors confirm a strong interaction between the silane and MgCl2. © 1993 John Wiley & Sons, Inc.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/pola.1993.080311121

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