Electronic Resource
Springer
Chemistry of heterocyclic compounds
9 (1973), S. 1240-1243
ISSN:
1573-8353
Source:
Springer Online Journal Archives 1860-2000
Topics:
Chemistry and Pharmacology
Notes:
Abstract It is shown that it is possible to synthesize 1-acyl-4-methyl-7-azatryptamines from ethyl (4-methyl-7-aza-3-indolyl)acetate through 3-(β-chloroethyl)-4-methyl-7-azaindole with subsequent acylation by replacement of halogen by a nitro group and reduction. The N-acetyl group is cleaved in the reaction of 1-acetyl-3-(β-chloroethyl)-4-methyl-7-azaindole with ammonia, bis (dimethylmethoxysilyl)amide potassium salt, and potassium phthalimide (with subsequent removal of the phthalimide protective group).
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF00477460
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