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Structure of a novel fluxional molecule: 1,2,3-trithia-[3]-ferrocenophane (1972)

Davis, Betty R. ; Bernal, Ivan

Springer

Journal of chemical crystallography 2 (1972), S. 107-114

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ISSN: 1572-8854

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract The crystal and molecular structure of 1,2,3-trithia-[3]-ferrocenophane has been determined from three-dimensional X-ray data collected by counter techniques. The molecule consists of two nearly parallel, eclipsed cyclopentadienyl rings linked by an S3 bridge. The material crystallizes in the monoclinic space groupP21/c with unit cell parametersa = 9·628(3),b = 9·347(4),c= 11·408(4) Å, β = 96·70(3) °. The structure was solved by standard techniques and the least-squares refinement converged to a conventionalR factor of 9·6 %.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01464791

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