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Mass spectral determination of aldehydes, ketones, and carboxylic acids using 1,1-dimethylhydrazine (1985)

McDaniel, C. A. ; Howard, Ralph W.

Springer

Journal of chemical ecology 11 (1985), S. 303-310

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ISSN: 1573-1561

Keywords: Semiochemicals ; pheromones ; methyl esters ; N,N-dimethylhydrazones ; N,N-dimethylhydrazine ; mass spectrometry

Source: Springer Online Journal Archives 1860-2000

Topics: Biology , Chemistry and Pharmacology

Notes: Abstract Analyses of nanogram to milligram quantities of aliphatic aldehydes, fatty acids, and unhindered aliphatic ketones such as those typically found in pheromonal blends have been effected by treating these mixtures with 1,1-dimethylhydrazine. The aldehydes and ketones formN,N-dimethylhydrazones, while the fatty acids form methyl esters. Structural elucidation of the reaction products was achieved using EI and CI gas chromatography-mass spectrometry.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01411416

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