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Ramanspektroskopische Untersuchungen an PCl5 II. Das System PCl5—ZrCl4 (1980)

Demiray, A. Fezâ ; Brockner, Wolfgang

Springer

Monatshefte für Chemie 111 (1980), S. 21-27

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ISSN: 1434-4475

Keywords: Melt ; PCl5−ZrCl4 ; Raman spectra ; Solid

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Abstract Raman spectra of some solid and molten PCl5−ZrCl4 mixtures have been recorded. ZrCl6 2− complex ions accompanied by at least one more chlorozirconate species are present in the solid as well as in the melt. The newRaman frequencies are attributed to ZrCl5 −, which fundamentals are given and assignment is proposed to be analogous to TiCl5 −. The presence of ZrCl6 2− and ZrCl5 − can be explained by the equilibrium ZrCl6 2−+PCl4 +⇌ZrCl5 −+PCl5.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00938713

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