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  • 1
    Electronic Resource
    Electronic Resource
    Resolution of the enantiomers of verapamil and gallopamil by chiral liquid chromatography-mass spectrometry (1997)
    Springer
    Chromatographia 44 (1997), S. 477-483 
    Details
    ISSN: 1612-1112
    Keywords: Column liquid chromatography ; Chiral separations ; Calcium channel antagonists ; On-line liquid chromatography-mass spectrometry
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary An HPLC-CSP method has been developed for the separation of enantiomers of verapamil and gallopamil using the improved version of the α1-acid glycoprotein, chiral stationary phase as selector with a volatile mobile phase. The results of the investigation provide the conditions which allow direct coupling to a mass spectrometer. In addition, the simultaneous enantioseparation of both the enantiomeric pairs of verapamil and gallopamil was achieved.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02466740
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