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Reduktion von Oximen mit Natriumboranat in Gegenwart von Übergangsmetallverbindungen (1984)

Ipaktschi, Junes

Weinheim : Wiley-Blackwell

Berichte der deutschen chemischen Gesellschaft 117 (1984), S. 856-858

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ISSN: 0009-2940

Keywords: Chemistry ; Inorganic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Reduction of Oximes with Sodium Borohydride in the Presence of Transition Metal CompoundsThe reduction of oximes with sodium borohydride in the presence of NiCl2 · 6 H2O and MoO3 was investigated. The combination of NaBH4 with NiCl2 · 6 H2O converted the unsaturated oximes through exhaustive reduction into saturated amines (Table 1). The C = C double bond remains preserved if the reduction is carried out in the presence of MoO3 (Table 2). The stereo-chemistry of the reduction in the presence of NiCl2 · 6 H2O is distinctivly different from that of MoO3.

Additional Material: 2 Tab.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/cber.19841170237

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