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An optical cell for photographic studies of gas evolution during molten salt electrolysis (1972)

King, P. L. ; Welch, B. J.

Springer

Journal of applied electrochemistry 2 (1972), S. 23-29

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ISSN: 1572-8838

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology , Electrical Engineering, Measurement and Control Technology

Notes: Abstract The simple optical cell described is useful for providing supplementary information on the evolution of gases during the electrolysis of fused salts or other electrolytes. Its use with PbS-PbCl2 and PbS-PbCl2-NaCl melts demonstrated that, for anodic sulphur gas production, residual gas evolution occurs, indicating the formation of a chemisorbed species as a reaction intermediate. Dissolution of the sulphur in the melt also takes place; its rate increases with increase in temperature and sulphide concentration.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00615188

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